4-(Tetrahydropyran-4-yloxy)benzaldehyde synthesis
- Product Name:4-(Tetrahydropyran-4-yloxy)benzaldehyde
- CAS Number:215460-40-5
- Molecular formula:C12H14O3
- Molecular Weight:206.24
123-08-0
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215460-40-5
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Yield:-
Steps:
R.15 4-[(Oxan-4-yl)oxy]benzaldehyde
Reference Example 15
4-[(Oxan-4-yl)oxy]benzaldehyde
The compound obtained in step 1 of Reference Example 14 (1.2 g) and 4-hydroxybenzaldehyde (700 mg) were used as manufacturing raw materials, and the same procedure as that in step 2 of Reference Example 14 was performed to obtain the title compound (828 mg) as a solid.
1H-NMR (CDCl3) δ: 1.78-1.88 (2H, m), 2.02-2.10 (2H, m), 3.58-3.66 (2H, m), 3.96-4.03 (2H, m), 4.58-4.68 (1H, m), 7.01 (2H, d, J=7.9 Hz), 7.84 (2H, d, J=7.9 Hz), 9.88 (1H, s).
References:
US2022/185815,2022,A1
2081-44-9
291 suppliers
$6.00/1g
123-08-0
901 suppliers
$5.00/10g
215460-40-5
29 suppliers
$110.00/50mg