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7459-73-6

(4-Vinylphenyl)chloromagnesium synthesis

2synthesis methods
-

Yield:-

Reaction Conditions:

with magnesium in tetrahydrofuran;

Steps:

R.2 Synthesis of (4-vinylphenyl)dimethylchlorosilane

REFERENCE EXAMPLE 2 Synthesis of (4-vinylphenyl)dimethylchlorosilane (4-Vinylphenyl)magnesium chloride was synthesised by the gradual dropwise addition of 50 parts of p-chlorostyrene to a mixture of 15 parts magnesium turnings and 100 parts tetrahydrofuran. This was gradually added dropwise over 2 hours to 50 parts of dimethyldichlorosilane dissolved in 100 parts tetrahydrofuran, after which the reaction was heated for an additional 1 hour under reflux.

References:

US5502229,1996,A