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Bicyclo[4.1.0]hept-4-en-3-ol, 4,7,7-trimethyl-, (1R,3R,6S)- synthesis

8synthesis methods
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Yield:4017-81-6 16 % Chromat. ,4017-82-7 0.5 % Chromat. ,4017-83-8 77 % Chromat.

Reaction Conditions:

with aluminum isopropoxide in toluene; for 3 h;Heating;Title compound not separated from byproducts;

References:

Ruecker, Gerhard;Frey, Klaus [Liebigs Annalen der Chemie,1987,p. 389 - 392]