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ChemicalBook CAS DataBase List 9-Octyl-2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
406726-92-9

9-Octyl-2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 82 percent / K2CO3 / dimethylformamide / 12 h / 80 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 - 0 °C
2.2: 67 percent / tetrahydrofuran; hexane / 12 h / -78 - 20 °C

References:

Bouchard, Jimmy;Wakim, Salem;Leclerc, Mario [Journal of Organic Chemistry,2004,vol. 69,# 17,p. 5705 - 5711]

FullText

9-Octyl-2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole Related Search: