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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

Ethyl 3,4,6-Tri-O-acetyl-2-acetamido-2-deoxy-β-D-thioglucopyranoside synthesis

5synthesis methods
D-arabino-Hex-1-enitol, 1,5-anhydro-2-deoxy-3,6-bis-O-(phenylmethyl)-, 4-acetate

165524-87-8
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Ethyl 3,4,6-Tri-O-acetyl-2-acetamido-2-deoxy-β-D-thioglucopyranoside

4239-72-9
22 suppliers
$52.50/250mg

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: bisdicollidine iodonium perchloride
1.2: 68 percent / LiHMDS
2.1: Na; NH3
3.1: methanol

References:

Wang, Zhi-Guang;Zhang, XuFang;Live, David;Danishefsky, Samuel J. [Angewandte Chemie - International Edition in English,2000,vol. 39,# 20,p. X3652-3656]

β-D-Glucopyranoside, ethyl 2-amino-2-deoxy-1-thio-, 3,4,6-triacetate

3945-29-7
1 suppliers
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Acetic anhydride

108-24-7
5 suppliers
$14.00/250ML

Ethyl 3,4,6-Tri-O-acetyl-2-acetamido-2-deoxy-β-D-thioglucopyranoside

4239-72-9
22 suppliers
$52.50/250mg

References
NSC170116

6838-16-0
3 suppliers
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α-D-Glucofuranoside, ethyl 2-(acetylamino)-2-deoxy-1-thio-

38859-04-0
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Ethyl 3,4,6-Tri-O-acetyl-2-acetamido-2-deoxy-β-D-thioglucopyranoside

4239-72-9
22 suppliers
$52.50/250mg

References
β-D-Glucopyranoside, ethyl 2-deoxy-3,6-bis-O-(phenylmethyl)-2-[(phenylsulfonyl)amino]-1-thio-, 4-acetate

187879-61-4
0 suppliers
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Ethyl 3,4,6-Tri-O-acetyl-2-acetamido-2-deoxy-β-D-thioglucopyranoside

4239-72-9
22 suppliers
$52.50/250mg

References
Acetic anhydride

108-24-7
5 suppliers
$14.00/250ML

β-D-Glucopyranoside, ethyl 2-amino-2-deoxy-1-thio-

312967-20-7
0 suppliers
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Ethyl 3,4,6-Tri-O-acetyl-2-acetamido-2-deoxy-β-D-thioglucopyranoside

4239-72-9
22 suppliers
$52.50/250mg

References