ChemicalBook CAS DataBase List N-[5-(4-bromophenyl)-6-chloro-4-pyrimidinyl]-N'-benzyl-sulfamide

N-[5-(4-bromophenyl)-6-chloro-4-pyrimidinyl]-N'-benzyl-sulfamide synthesis

7synthesis methods

Product Name:N-[5-(4-bromophenyl)-6-chloro-4-pyrimidinyl]-N'-benzyl-sulfamide
CAS Number:441797-42-8
Molecular formula:C17H14BrClN4O2S
Molecular Weight:453.74

100-46-9 Synthesis

100-46-9
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N-[5-(4-bromophenyl)-6-chloro-4-pyrimidinyl]-N'-benzyl-sulfamide

441797-42-8
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: dichloromethane / 1 h / 0 - 20 °C
1.2: 11 h / 0 - 20 °C
2.1: hydrogenchloride / 1,4-dioxane / 9 h / 20 °C
3.1: potassium tert-butylate / methanol / 0.25 h / 20 °C
4.1: dimethyl sulfoxide / 24 h / 20 °C

References:

US2012/142716,2012,A1

41841-16-1 Synthesis

41841-16-1
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441797-42-8
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References

1878-68-8 Synthesis

1878-68-8
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$6.00/10g

441797-42-8
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References

149506-35-4 Synthesis

2-(4-BROMOPHENYL)-PROPANEDIOIC ACID, 1,3-MDIETHYL ESTER

149506-35-4
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$43.00/250mg

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References

706811-25-8 Synthesis

4(1H)-PyriMidinone, 5-(4-broMophenyl)-6-hydroxy-

706811-25-8
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$12.00/1g

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References