1,3-Cyclohexadiene, 1-(1,5-dimethyl-4-hexen-1-yl)-4-methyl- synthesis

3synthesis methods

Product Name:1,3-Cyclohexadiene, 1-(1,5-dimethyl-4-hexen-1-yl)-4-methyl-
CAS Number:451-55-8
Molecular formula:C15H24
Molecular Weight:204.35

2-Cyclohexen-1-one, 3-(1,5-dimethyl-4-hexenyl)-

72055-87-9
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1,3-Cyclohexadiene, 1-(1,5-dimethyl-4-hexen-1-yl)-4-methyl-

451-55-8
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) LDA / 1.) THF, hexane, 45 min, -78 deg C 2.) THF, 4 h, -78 deg C to RT; 12 h, RT
2: 76 percent / NaBH₄ / methanol / 1.) 30 min, 0 deg C, 2.) 5 h, RT
3: Et₃N(+)SO₂N(-)CO₂Me / benzene

References:

Weyerstahl, Peter;Marschall-Weyerstahl, Helga;Scholz, Stefan [Liebigs Annalen der Chemie,1986,# 6,p. 1021 - 1029]

3-Cyclohexen-1-ol, 4-(1,5-dimethyl-4-hexen-1-yl)-1-methyl-

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451-55-8
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644-30-4 Synthesis

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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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451-55-8
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References