N-[4-[(Trifluoroacetyl)amino]benzoyl-d4]-L-glutamic Acid Dimethyl Ester synthesis
- Product Name:N-[4-[(Trifluoroacetyl)amino]benzoyl-d4]-L-glutamic Acid Dimethyl Ester
- CAS Number:461426-33-5
- Molecular formula:C16H17F3N2O6
- Molecular Weight:390.32
150-13-0
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: 58.1 percent / deuterium oxide; Pd/C / 2 h / 200 °C
2.1: 2 h / 20 °C
3.1: dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / tetrahydrofuran / 0.5 h / 20 °C
3.2: diisopropylethylamine / tetrahydrofuran / 4 h / 20 °C
References:
Freisleben, Achim;Schieberle, Peter;Rychlik, Michael [Journal of Agricultural and Food Chemistry,2002,vol. 50,# 17,p. 4760 - 4768]