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ChemicalBook CAS DataBase List 6-AMINO-6-DEOXY-1,2:3,4-DI-O-ISOPROPYLIDENE-D-GALACTOPYRANOSIDE
4711-01-7

6-AMINO-6-DEOXY-1,2:3,4-DI-O-ISOPROPYLIDENE-D-GALACTOPYRANOSIDE synthesis

8synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 67 percent / Me2SO; (COCl)2; Et3N / CH2Cl2 / -70 °C
2: 76 percent / NH2OH*HCl; NaOAc / methanol; H2O / 24 h / 20 °C
3: 69 percent / LiAlH4 / diethyl ether / 2 h / 20 °C

References:

Streicher, Benedikt;Wuensch, Bernhard [Carbohydrate Research,2003,vol. 338,# 22,p. 2375 - 2385]