1-(1,1-dioxidotetrahydro-2H-thiopyran-4-yl)ethanone synthesis
- Product Name:1-(1,1-dioxidotetrahydro-2H-thiopyran-4-yl)ethanone
- CAS Number:473254-30-7
- Molecular formula:C7H12O3S-2
- Molecular Weight:176.2334
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 16 h / 20 °C
2: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
References:
WO2021/62089,2021,A1