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Thiophene, 3,3'-(1-cyclopentene-1,2-diyl)bis[2-methyl-5-phenyl- synthesis

3synthesis methods
Boronic acid, B,B'-[1-cyclopentene-1,2-diylbis(5-methyl-4,2-thiophenediyl)]bis-, B,B,B',B'-tetrabutyl ester

509083-61-8
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Thiophene, 3,3'-(1-cyclopentene-1,2-diyl)bis[2-methyl-5-phenyl-

473463-85-3
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Yield:473463-85-3 70%

Reaction Conditions:

with tetrakis(triphenylphosphine) palladium(0);sodium carbonate;ethylene glycol in tetrahydrofuran;hexane; for 2 h;Heating;Suzuki cross-coupling;

References:

De Jong, Jaap J. D.;Lucas, Linda N.;Hania, Ralph;Pugzlys, Audrius;Kellogg, Richard M.;Feringa, Ben L.;Duppen, Koos;Van Esch, Jan H. [European Journal of Organic Chemistry,2003,# 10,p. 1887 - 1893]

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