![](/CAS/20210111/GIF/475160-89-5.gif)
Carbamic acid, N-[[4-(hydroxymethyl)phenyl]methyl]-, 9H-fluoren-9-ylmethyl ester synthesis
- Product Name:Carbamic acid, N-[[4-(hydroxymethyl)phenyl]methyl]-, 9H-fluoren-9-ylmethyl ester
- CAS Number:475160-89-5
- Molecular formula:C23H21NO3
- Molecular Weight:359.42
![4-(FMOC-AMINOMETHYL)BENZOIC ACID](/CAS/GIF/164470-64-8.gif)
164470-64-8
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$9.00/1g
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Yield:475160-89-5 70%
Reaction Conditions:
Stage #1: N-(9-fluorenylmethyloxycarbonyl)-4-(aminomethyl)benzoic acidwith chloroformic acid ethyl ester;triethylamine in tetrahydrofuran at -7; for 1 h;
Stage #2: with sodium tetrahydroborate in methanol at 10; for 2.5 h;Further stages.;
References:
Sternson;Wong;Grozinger;Schreiber [Organic letters,2001,vol. 3,# 26,p. 4239 - 4242]
![4-(Aminomethyl)benzoic acid](/CAS/GIF/56-91-7.gif)
56-91-7
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$5.00/1g
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![N-(9-Fluorenylmethoxycarbonyloxy)succinimide](/CAS/GIF/82911-69-1.gif)
82911-69-1
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$7.00/25g
![Carbamic acid, N-[[4-(hydroxymethyl)phenyl]methyl]-, 9H-fluoren-9-ylmethyl ester](/CAS/20210111/GIF/475160-89-5.gif)
475160-89-5
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