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9-(2-Ethylhexyl)-2,7-bis(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole synthesis
- Product Name:9-(2-Ethylhexyl)-2,7-bis(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
- CAS Number:476360-83-5
- Molecular formula:C32H47B2NO4
- Molecular Weight:531.34
![2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane](/CAS/GIF/61676-62-8.gif)
61676-62-8
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$11.19/5G
![2,7-DibroMo-9-(2-ethylhexyl)-9H-carbazole](/CAS/20150408/GIF/544436-46-6.gif)
544436-46-6
49 suppliers
$60.00/5mg
![9-(2-Ethylhexyl)-2,7-bis(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole](/CAS/20150408/GIF/476360-83-5.gif)
476360-83-5
41 suppliers
$136.00/200MG
Yield:476360-83-5 84 %
Reaction Conditions:
Stage #1: 2,7-dibromo-9-(2-ethylhexyl)-9H-carbazolewith n-butyllithium in tetrahydrofuran;hexane at -78;Schlenk technique;Inert atmosphere;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran;hexane at -78;Schlenk technique;Inert atmosphere;
References:
Lucas, Fabien;Rault-Berthelot, Jo?lle;Quinton, Cassandre;Poriel, Cyril [Journal of Materials Chemistry C,2022,vol. 10,# 37,p. 14000 - 14009] Location in patent:supporting information
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![2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane](/CAS/GIF/61676-62-8.gif)
61676-62-8
311 suppliers
$11.19/5G
![9-(2-Ethylhexyl)-2,7-bis(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole](/CAS/20150408/GIF/476360-83-5.gif)
476360-83-5
41 suppliers
$136.00/200MG
![Bis(pinacolato)diboron](/CAS/20180808/GIF/73183-34-3.gif)
73183-34-3
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$6.00/5g
![2,7-DibroMo-9-(2-ethylhexyl)-9H-carbazole](/CAS/20150408/GIF/544436-46-6.gif)
544436-46-6
49 suppliers
$60.00/5mg
![9-(2-Ethylhexyl)-2,7-bis(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole](/CAS/20150408/GIF/476360-83-5.gif)
476360-83-5
41 suppliers
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![9H-Carbazole-2,7-diamine](/CAS/GIF/6402-13-7.gif)
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![9-(2-Ethylhexyl)-2,7-bis(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole](/CAS/20150408/GIF/476360-83-5.gif)
476360-83-5
41 suppliers
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![9-(2-Ethylhexyl)-2,7-bis(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole](/CAS/20150408/GIF/476360-83-5.gif)
476360-83-5
41 suppliers
$136.00/200MG