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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 2-Butylsulfanyl-thiocarbonylsulfanyl-propionic acid

2-Butylsulfanyl-thiocarbonylsulfanyl-propionic acid synthesis

1synthesis methods
Carbon disulfide

75-15-0
237 suppliers
$40.00/100g

Butanethiol

109-79-5
224 suppliers
$14.00/25g

598-72-1 Synthesis
2-Bromopropionic acid

598-72-1
341 suppliers
$16.00/25g

2-Butylsulfanyl-thiocarbonylsulfanyl-propionic acid

480436-46-2
11 suppliers
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Yield:480436-46-2 81%

Reaction Conditions:

Stage #1: carbon disulfide;1-butanethiolwith sodium hydroxide in acetone at 20; for 0.5 h;
Stage #2: 2-Bromopropionic acidwith sodium hydroxide in acetone at 20; for 24 h;

References:

Ferguson, Christopher J.;Hughes, Robert J.;Nguyen, Duc;Pham, Binh T.T.;Gilbert, Robert G.;Serelis, Algirdas K.;Such, Christopher H.;Hawkett, Brian S. [Macromolecules,2005,vol. 38,# 6,p. 2191 - 2204]