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ChemicalBook CAS DataBase List (4S 4'S)-(-)-2 2'-(3-PENTYLIDENE)BIS(4-&
160191-65-1

(4S 4'S)-(-)-2 2'-(3-PENTYLIDENE)BIS(4-& synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 17.25 h / 0 °C / Inert atmosphere; Reflux
2: triethylamine / dichloromethane / 2 h / 0 - 20 °C
3: triethylamine; dmap; p-toluenesulfonyl chloride / dichloromethane / 0 - 20 °C

References:

Li, Meiling;Hawkins, Alison;Barber, David M.;Bultinck, Patrick;Herrebout, Wouter;Dixon, Darren J. [Chemical Communications,2013,vol. 49,# 46,p. 5265 - 5267]

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