5-(3-chlorophenyl)thiophene-2-carboxylic acid synthesis

3synthesis methods

Product Name:5-(3-chlorophenyl)thiophene-2-carboxylic acid
CAS Number:893733-15-8
Molecular formula:C11H7ClO2S
Molecular Weight:238.69

5-Bromo-thiophene-2-carboxylic acid methyl ester

62224-19-5
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5-(3-chlorophenyl)thiophene-2-carboxylic acid

893733-15-8
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: Na₂CO₃ / Pd(PPh₃)4 / 1,2-dimethoxy-ethane / 100 °C
2: aq. LiOH / tetrahydrofuran

References:

Denonne, Frederic;Binet, Sophie;Burton, Maggi;Collart, Philippe;Dipesa, Alan;Ganguly, Tanmoy;Giannaras, Alexander;Kumar, Seema;Lewis, Timothy;Maounis, Florence;Nicolas, Jean-Marie;Mansley, Tamsin;Pasau, Patrick;Preda, Dorin;Stebbins, Karin;Volosov, Alexander;Zou, Dong [Bioorganic and Medicinal Chemistry Letters,2007,vol. 17,# 12,p. 3258 - 3261]

63503-60-6 Synthesis

63503-60-6
423 suppliers
$9.00/1g

893733-15-8
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References

62224-19-5
144 suppliers
$11.00/1g

63503-60-6 Synthesis

63503-60-6
423 suppliers
$9.00/1g

893733-15-8
6 suppliers
inquiry

References