[5-(4-fluorophenyl)-2-Methyl-furan-3-yl]Methanol synthesis

3synthesis methods

Product Name:[5-(4-fluorophenyl)-2-Methyl-furan-3-yl]Methanol
CAS Number:111787-93-0
Molecular formula:C12H11FO2
Molecular Weight:206.21

403-29-2 Synthesis

403-29-2
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$8.00/5g

[5-(4-fluorophenyl)-2-Methyl-furan-3-yl]Methanol

111787-93-0
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) sodium pellets / 1.) toluene, room temp., 3 days, 2.) toluene, 0 deg C, 1 h then room temp., 1 day
2: 60 percent / 12 M hydrochloric acid / ethanol / 24 h / Heating
3: 75 percent / lithium aluminum hydride / tetrahydrofuran / 24 h / Heating

References:

Porretta;Scalzo;Chimenti;Bolasco;Biava;Fischetti;Riccardi [Farmaco, Edizione Scientifica,1987,vol. 42,# 5,p. 629 - 639]

Methyl 5-(4-fluorophenyl)-2-Methylfuran-3-carboxylate

444914-29-8
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111787-93-0
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References

ETHYL 5-(4-FLUOROPHENYL)-2-METHYL-3-FUROATE

111787-83-8
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$282.75/1g

111787-93-0
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References