5-(4-METHOXY-BENZYL)-[1,3,4]THIADIAZOL-2-YLAMINE synthesis
- Product Name:5-(4-METHOXY-BENZYL)-[1,3,4]THIADIAZOL-2-YLAMINE
- CAS Number:63617-18-5
- Molecular formula:C10H11N3OS
- Molecular Weight:221.28
104-01-8
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$6.00/10g
79-19-6
494 suppliers
$14.00/1g
63617-18-5
23 suppliers
$155.00/500mg
Yield:63617-18-5 90%
Reaction Conditions:
Stage #1: 4-Methoxyphenylacetic acid;thiosemicarbazidewith trichlorophosphate for 0.75 h;Reflux;
Stage #2: with water for 4 h;Reflux;
Stage #3: with potassium hydroxide in water;Cooling;
References:
Badiger, Naveenkumar P.;Shetty, Nitinkumar S.;Lamani, Ravi S.;Khazi, Imtiyaz Ahmed M. [Heterocyclic Communications,2009,vol. 15,# 6,p. 433 - 442] Location in patent:experimental part
79-19-6
494 suppliers
$14.00/1g
4693-91-8
90 suppliers
$19.00/1g
63617-18-5
23 suppliers
$155.00/500mg