ChemicalBook CAS DataBase List 5-AMINO-3-THIOXO-3H-(1,2)DITHIOLE-4-CARBONITRILE

5-AMINO-3-THIOXO-3H-(1,2)DITHIOLE-4-CARBONITRILE synthesis

1synthesis methods

Product Name:5-AMINO-3-THIOXO-3H-(1,2)DITHIOLE-4-CARBONITRILE
CAS Number:5147-74-0
Molecular formula:C4H2N2S3
Molecular Weight:174.27

2,2-Bis(potassiothio)ethene-1,1-dicarbonitrile

4777-48-4
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5-AMINO-3-THIOXO-3H-(1,2)DITHIOLE-4-CARBONITRILE

5147-74-0
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Yield:5147-74-0 21%

Reaction Conditions:

with tetraethylammonium iodide;niobium pentachloride in ethanol;ethylene glycol at 20; for 0.5 h;

References:

Cao, Yanning;Zhang, Hanhui;Lin, Yiji;Huang, Changcang;Chen, Yiping;Zhang, Fengli;Chen, Jianshan [Journal of Molecular Structure,2008,vol. 888,# 1-3,p. 354 - 359] Location in patent:experimental part