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ChemicalBook CAS DataBase List 5-BROMO-2-IODOBENZOTRIFLUORIDE
364-12-5

5-BROMO-2-IODOBENZOTRIFLUORIDE synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: KBr; NaBO3*4H2O; AcOH / (NH4)6Mo7O24*4H2O / 3 h / 20 °C
2: 2.73 g / I2; tert-butyl nitrite / acetonitrile / 16 h / 20 °C

References:

Hattori, Yoshihide;Yamamoto, Hitoshi;Ando, Hideya;Kondoh, Hirofumi;Asano, Tomoyuki;Kirihata, Mitsunori;Yamaguchi, Yoshihiro;Wakamiya, Tateaki [Bioorganic and Medicinal Chemistry,2007,vol. 15,# 5,p. 2198 - 2205]

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