5-Bromo-2-isopropyl-2,3-dihydro-isoindol-1-one synthesis
- Product Name:5-Bromo-2-isopropyl-2,3-dihydro-isoindol-1-one
- CAS Number:864866-47-7
- Molecular formula:C11H12BrNO
- Molecular Weight:254.12
888030-75-9
4 suppliers
inquiry
888030-82-8
2 suppliers
inquiry
864866-47-7
24 suppliers
$207.90/250mg
Yield:864866-47-7 90%
Reaction Conditions:
Stage #1: N-isopropyl-4-bromo-2-hydroxymethylbenzamidewith isopropylmagnesium chloride in tetrahydrofuran at 20; for 0.5 h;
Stage #2: with N,N,N',N'-Tetramethylphosphorodiamidic chloride in tetrahydrofuran at 20; for 14 h;
References:
Tsuritani, Takayuki;Kii, Satoshi;Akao, Atsushi;Sato, Kimihiko;Nonoyama, Nobuaki;Mase, Toshiaki;Yasuda, Nobuyoshi [Synlett,2006,# 5,p. 801 - 803]
75-31-0
437 suppliers
$14.00/25mL
78471-43-9
223 suppliers
$6.00/250mg
864866-47-7
24 suppliers
$207.90/250mg
888030-75-9
4 suppliers
inquiry
864866-47-7
24 suppliers
$207.90/250mg
888030-82-8
2 suppliers
inquiry
864866-47-7
24 suppliers
$207.90/250mg
64169-34-2
359 suppliers
$12.00/5G
864866-47-7
24 suppliers
$207.90/250mg