5-BROMO-3-PHENYL-1H-INDAZOLE synthesis

2synthesis methods

Product Name:5-BROMO-3-PHENYL-1H-INDAZOLE
CAS Number:57639-16-4
Molecular formula:C13H9BrN2
Molecular Weight:273.13

Phenol, 4-(5-bromo-3-phenyl-2H-indazol-2-yl)-2,6-dimethyl-

1431709-02-2
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57639-16-4
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Yield:57639-16-4 87%

Reaction Conditions:

Stage #1: 4-(5-bromo-3-phenyl-2H-indazol-2-yl)-2,6-dimethylphenol in methanol at 0; for 0.166667 h;Inert atmosphere;
Stage #2: with ammonium cerium (IV) nitrate in methanol; for 0.25 h;Inert atmosphere;

References:

Lian, Yajing;Bergman, Robert G.;Lavis, Luke D.;Ellman, Jonathan A. [Journal of the American Chemical Society,2013,vol. 135,# 19,p. 7122 - 7125] Location in patent:supporting information

Methanone, (5-bromo-2-fluorophenyl)phenyl-

885124-16-3
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57639-16-4
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References

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5-BROMO-3-METHYL-1H-INDAZOLE