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5-(Bromomethyl)-2,4,6-trichloropyrimidine synthesis

1synthesis methods
-

Yield:1780-37-6 90%

Reaction Conditions:

with N-Bromosuccinimide;2,2'-azobis(isobutyronitrile) in tetrachloromethane; for 36 h;Heating;

References:

Ye, Chengfeng;Gao, Haixiang;Boatz, Jerry A.;Drake, Gregory W.;Twamley, Brendan;Shreeve, Jean'ne M. [Angewandte Chemie - International Edition,2006,vol. 45,# 43,p. 7262 - 7265]