![](/CAS/GIF/117052-19-4.gif)
(5''-CHLORO-2'',3''-DIMETHOXY)ACETOPHENONE synthesis
- Product Name:(5''-CHLORO-2'',3''-DIMETHOXY)ACETOPHENONE
- CAS Number:117052-19-4
- Molecular formula:C10H11ClO3
- Molecular Weight:214.65
![1-(5-CHLORO-2,3-DIMETHOXYPHENYL)ETHANOL](/CAS/GIF/117052-18-3.gif)
117052-18-3
6 suppliers
inquiry
![(5''-CHLORO-2'',3''-DIMETHOXY)ACETOPHENONE](/CAS/GIF/117052-19-4.gif)
117052-19-4
17 suppliers
$90.00/50mg
Yield:117052-19-4 96%
Reaction Conditions:
with manganese(IV) oxide in chloroform; for 8 h;Reflux;
Steps:
5
Example 5; The synthesis of ketone 3 was carried out by reducting the commercially available aldehyde 1 to the corresponding alcohol 2 following the procedure disclosed in WO06/081332A1, followed by the oxidation to ketone 3 with MnO2 with a good yield (Scheme 8).
References:
EP2103596,2009,A1 Location in patent:Page/Page column 50
![5-CHLORO-2 3-DIMETHOXYBENZALDEHYDE](/CAS/GIF/86232-28-2.gif)
86232-28-2
62 suppliers
$21.00/250mg
![(5''-CHLORO-2'',3''-DIMETHOXY)ACETOPHENONE](/CAS/GIF/117052-19-4.gif)
117052-19-4
17 suppliers
$90.00/50mg