5-CHLORO-2-METHYL-NICOTINIC ACID METHYL ESTER synthesis
- Product Name:5-CHLORO-2-METHYL-NICOTINIC ACID METHYL ESTER
- CAS Number:350597-49-8
- Molecular formula:C8H8ClNO2
- Molecular Weight:185.61
105-45-3
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350597-49-8
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: t-BuOK / tetrahydrofuran / 0.75 h / 20 °C
1.2: 86 percent / DABCO / 3 h / 45 °C
2.1: 95 percent Chromat. / NH4OAc / tetrahydrofuran / 6 h / Heating
References:
Marcoux;Marcotte;Wu;Dormer;Davies;Hughes;Reider [Journal of Organic Chemistry,2001,vol. 66,# 12,p. 4194 - 4199]
325855-84-3
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350597-49-8
101 suppliers
$29.00/250mg