5-Chlorohex-5-enenitrile synthesis
- Product Name:5-Chlorohex-5-enenitrile
- CAS Number:951887-60-8
- Molecular formula:C6H8ClN
- Molecular Weight:129.59
14918-21-9
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Yield:951887-60-8 98%
Reaction Conditions:
with hydrogenchloride;chloro(1,5-cyclooctadiene)(pentamethylcyclopentadiene)ruthenium(II);triphenylphosphine in diethyl ether;1,2-dichloro-ethane at 20; for 0.166667 h;Inert atmosphere;Schlenk technique;
References:
Dérien, Sylvie;Klein, Hubert;Bruneau, Christian [Angewandte Chemie - International Edition,2015,vol. 54,# 41,p. 12112 - 12115][Angew. Chem.,2015,vol. 127,p. 12280 - 12283,4] Location in patent:supporting information