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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

5-DIMETHYLAMINO-2-HYDROXY-3-METHOXYBENZALDEHYDE synthesis

1synthesis methods
50-00-0 Synthesis
Formaldehyde

50-00-0
847 suppliers
$10.00/25g

2-HYDROXY-3-METHOXY-5-NITROBENZALDEHYDE

17028-61-4
108 suppliers
$18.00/1g

5-DIMETHYLAMINO-2-HYDROXY-3-METHOXYBENZALDEHYDE

262614-68-6
16 suppliers
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Yield:262614-68-6 75%

Reaction Conditions:

with palladium 10% on activated carbon;hydrogen in ethanol;water at 20; under 750.075 Torr; for 24 h;Inert atmosphere;

References:

Waibel, Michael;Hasserodt, Jens [Tetrahedron Letters,2009,vol. 50,# 23,p. 2767 - 2769] Location in patent:supporting information; experimental part