5-fluoro-6-Methoxy-1H-indole-2-carboxylic acid synthesis
- Product Name:5-fluoro-6-Methoxy-1H-indole-2-carboxylic acid
- CAS Number:136818-65-0
- Molecular formula:C10H8FNO3
- Molecular Weight:209.17
351-54-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: sodium methylate / methanol / 19 h / -10 - 20 °C
2: toluene / 4 h / Reflux
3: potassium hydroxide / water; 1,4-dioxane / 3 h / 50 °C
References:
CoMentis, Inc.;BILCER, Geoffrey M.;NG, Raymond US2016/9706, 2016, A1