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ChemicalBook CAS DataBase List 5-hydroxyisophthaldiamide
68052-43-7

5-hydroxyisophthaldiamide synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: thionyl chloride / tetrahydrofuran; N,N-dimethyl-formamide / Schlenk technique; Reflux
2: ammonium hydroxide / tetrahydrofuran / -40 °C

References:

Harloff, Joerg;Karsch, Markus;Lund, Henrik;Schulz, Axel;Villinger, Alexander [Zeitschrift fur Anorganische und Allgemeine Chemie,2014,vol. 640,# 7,p. 1330 - 1341]