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ChemicalBook CAS DataBase List (5-Hydroxypentyloxy)-acetic acid tert-butyl ester
144682-02-0

(5-Hydroxypentyloxy)-acetic acid tert-butyl ester synthesis

5synthesis methods
1-Pentanol, 5-[(tetrahydro-2H-pyran-2-yl)oxy]-

76102-74-4
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(5-Hydroxypentyloxy)-acetic acid tert-butyl ester

144682-02-0
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inquiry

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 77 percent / 50percent aq. NaOH, tetrabutylammonium hydrogen sulfate / CH2Cl2 / 12 h / Ambient temperature
2: 61 percent / p-TsOH / methanol

References:

Nagatsuki, Fumi;Sasaki, Shigeki;Maeda, Minoru [Journal of Fluorine Chemistry,1992,vol. 56,# 3,p. 373 - 383]