ChemicalBook CAS DataBase List 5-IODO-1-METHYL-1H-PYRAZOLE

5-IODO-1-METHYL-1H-PYRAZOLE synthesis

2synthesis methods

Product Name:5-IODO-1-METHYL-1H-PYRAZOLE
CAS Number:34091-51-5
Molecular formula:C4H5IN2
Molecular Weight:208

930-36-9 Synthesis

930-36-9
326 suppliers
$5.00/1g

34091-51-5
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$15.00/1g

Yield: 92%

Reaction Conditions:

Stage #1:1-methyl-1H-pyrazole with (PMDETA)₂K₂Mg(CH₂SiMe₃)₄ at 0; for 2 h;Inert atmosphere;Schlenk technique;
Stage #2: with iodine for 1 h;Inert atmosphere;Schlenk technique;regioselective reaction;

References:

Baillie, Sharon E.;Bluemke, Tobias D.;Clegg, William;Kennedy, Alan R.;Klett, Jan;Russo, Luca;De Tullio, Marco;Hevia, Eva [Chemical Communications,2014,vol. 50,# 85,p. 12859 - 12862] Location in patent:supporting information

930-36-9 Synthesis

930-36-9
326 suppliers
$5.00/1g

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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inquiry

34091-51-5
107 suppliers
$15.00/1g

References

5-IODO-1-METHYL-1H-PYRAZOLE Related Search:

2-Hydroxy-5-iodo-3-methylpyridine 5-IODO-2-METHOXY-3-(TRIFLUOROMETHYL)-PYRIDINONE 5-iodo-4-(trifluoroMethyl)thiazol-2-aMine