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ChemicalBook CAS DataBase List 5-Iodo-4-methoxy-6-methylpyrimidine

5-Iodo-4-methoxy-6-methylpyrimidine synthesis

1synthesis methods
5-Iodo-4-methoxy-6-methylpyrimidine

107166-94-9
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acrylic acid methyl ester

292638-85-8
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2-Propenoic acid, 3-(4-methoxy-6-methyl-5-pyrimidinyl)-, methyl ester, (E)- (9CI)

107166-91-6
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Yield:107166-91-6 90%

Reaction Conditions:

with palladium diacetate;triethylamine;triphenylphosphine at 140; for 7 h;

References:

Wada, Akimori;Yamamoto, Junpei;Hase, Tetsuko;Nagai, Sotoo;Kanatomo, Shoichi [Synthesis,1986,# 7,p. 555 - 556]