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ChemicalBook CAS DataBase List 5-(Isopropylthio)-1,3,4-thiadiazol-2-amine
30062-47-6

5-(Isopropylthio)-1,3,4-thiadiazol-2-amine synthesis

3synthesis methods
-

Yield:30062-47-6 85%

Reaction Conditions:

Stage #1: 2-Amino-5-mercapto-1,3,4-thiadiazolewith potassium hydroxide in ethanol; for 0.166667 h;
Stage #2: isopropyl bromide in ethanol; for 2 h;

References:

Gao, Yaojun;Samanta, Sanjay;Cui, Taian;Lam, Yulin [ChemMedChem,2013,vol. 8,# 9,p. 1554 - 1560] Location in patent:supporting information