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5-Isoxazolamine,4-(3-pyridinyl)-(9CI) synthesis

3synthesis methods
3-Pyridineacetonitrile, α-[(dimethylamino)methylene]-

165404-42-2
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5-Isoxazolamine,4-(3-pyridinyl)-(9CI)

186960-06-5
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Yield:186960-06-5 52%

Reaction Conditions:

with hydroxylamine hydrochloride in acetic acid at 100; for 1 h;

References:

Olesen, Preben H.;Swedberg, Michael D. B.;Rimvall, Karin [Bioorganic and Medicinal Chemistry,1998,vol. 6,# 9,p. 1623 - 1629]