![](/CAS/20180703/GIF/881668-93-5.gif)
5-methoxyquinolin-3-amine synthesis
- Product Name:5-methoxyquinolin-3-amine
- CAS Number:881668-93-5
- Molecular formula:C10H10N2O
- Molecular Weight:174.2
![7-METHOXY-3-NITROQUINOLINE](/CAS/GIF/39977-95-2.gif)
39977-95-2
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![5-methoxyquinolin-3-amine](/CAS/20180703/GIF/881668-93-5.gif)
881668-93-5
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![3-QuinolinaMine, 7-Methoxy-](/CAS/GIF/87199-83-5.gif)
87199-83-5
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Yield: 12%
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in ethyl acetate at 20;
Steps:
20
0333] A mixture of 5- and 7-methoxy substituted 3-nitroquinolines (780 mg,3.82 mmol) was dissolved in EtOAc (75 mL) and the reaction mixture sparged with N2 for several minutes. 10% Pd/C (54 mg) was then added and a H2 balloon was connected to the reaction flask. The reaction mixture was sparged with H2 and stirred at room
References:
NOVARTIS AG WO2007/84786, 2007, A1 Location in patent:Page/Page column 117-118