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5-methyl-5H-thiophen-2-one synthesis

1synthesis methods
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Yield:7210-64-2 35% ,66372-83-6 24% ,3970-28-3 17% ,930-64-3 16%

Reaction Conditions:

with Lawessons reagent in toluene at 20 - 90; for 1.08333 h;Concentration;Temperature;Time;

References:

Li, Zheng;Tang, Xing;Jiang, Yetao;Zuo, Miao;Wang, Yangjun;Chen, Wei;Zeng, Xianhai;Sun, Yong;Lin, Lu [Green Chemistry,2016,vol. 18,# 10,p. 2971 - 2975]