5-propylindoline-2,3-dione synthesis
- Product Name:5-propylindoline-2,3-dione
- CAS Number:131609-60-4
- Molecular formula:C11H11NO2
- Molecular Weight:189.21
302-17-0
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$30.00/1mg
2696-84-6
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$108.00/5g
131609-60-4
21 suppliers
$220.00/100mg
Yield:131609-60-4 100%
Reaction Conditions:
Stage #1: chloral hydrate;4-propylanilinewith hydrogenchloride;hydroxylamine hydrochloride;sodium sulfate in water; for 0.0166667 h;Reflux;
Stage #2: with sulfuric acid at 50 - 80;
References:
Yoshino, Takamasa;Shibata, Koji;Wada, Hiroshi;Bando, Yoshimasa;Ishikawa, Ken;Takezoe, Hideo;Mori, Takehiko [Chemistry Letters,2009,vol. 38,# 3,p. 200 - 201] Location in patent:supporting information; experimental part