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5-(Pyridin-3-yl)pyrimidine synthesis

7synthesis methods
-

Yield:73082-69-6 87 %Spectr. ,56598-46-0 10%

Reaction Conditions:

with bis(η3-allyl-μ-chloropalladium(II));N,N,N′,N′-tetra(diphenylphosphinomethyl)-1,2-ethylenediamine;potassium carbonate in N,N-dimethyl acetamide;butan-1-ol at 110; for 20 h;Inert atmosphere;Suzuki Coupling;

References:

Wang, Kun;Fu, Qi;Zhou, Rong;Zheng, Xueli;Fu, Haiyan;Chen, Hua;Li, Ruixiang [Applied Organometallic Chemistry,2013,vol. 27,# 4,p. 232 - 238]