5-(TERT-BUTYL)-2-HYDROXYISOPHTHALIC ACID synthesis

4synthesis methods

Product Name:5-(TERT-BUTYL)-2-HYDROXYISOPHTHALIC ACID
CAS Number:157436-33-4
Molecular formula:C12H14O5
Molecular Weight:238.24

98-54-4
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5-(TERT-BUTYL)-2-HYDROXYISOPHTHALIC ACID

157436-33-4
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 34 percent / NaOH / H₂O / 96 h / Ambient temperature
2: 90 percent / K₂CO₃ / acetone / 18 h / Heating
3: 97 percent / NaOH, Adogen 464, KMnO₄ / H₂O / 50 degC, 1 h, reflux, 5 min
4: 77 percent / HBr / acetic acid / 0.17 h / 120 °C

References:

Fahrni, Christoph J.;Pfaltz, Andreas [Helvetica Chimica Acta,1998,vol. 81,# 3,p. 491 - 506]

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References

2203-14-7 Synthesis

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References

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References