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2-Oxazolidinone, 3-[6-[2-[(2,6-dichlorophenyl)Methoxy]ethoxy]hexyl]-5-(2,2-diMethyl-4H-1, 3-benzodioxin-6-yl)-, (5R)- synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: potassium tert-butylate / 1 h / 35 - 45 °C / Inert atmosphere
1.2: 1 h / 40 - 60 °C / Inert atmosphere
2.1: tetrabutylammomium bromide; sodium hydroxide / toluene; water / 20 h / 55 - 60 °C
3.1: potassium tert-butylate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
3.2: 3 h / 20 °C / Inert atmosphere

References:

PERRIGO API LTD.;Dammalapati, Venkata Lakshmi Narasimha Rao;Mudduluru, Hari Krishna;Aduri, Ravindra US2015/239862, 2015, A1

54030-34-1 Synthesis
Ethanone, 1-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)-

54030-34-1
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2-Oxazolidinone, 3-[6-[2-[(2,6-dichlorophenyl)Methoxy]ethoxy]hexyl]-5-(2,2-diMethyl-4H-1, 3-benzodioxin-6-yl)-, (5R)-

503068-36-8
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2-Oxazolidinone, 3-[6-[2-[(2,6-dichlorophenyl)Methoxy]ethoxy]hexyl]-5-(2,2-diMethyl-4H-1, 3-benzodioxin-6-yl)-, (5R)- Related Search: