1-(3-DIMETHYLAMINOMETHYL-4-METHOXY-PHENYL)-ETHANONE synthesis

5synthesis methods

Product Name:1-(3-DIMETHYLAMINOMETHYL-4-METHOXY-PHENYL)-ETHANONE
CAS Number:505070-85-9
Molecular formula:C12H17NO2
Molecular Weight:207.27

111-34-2 Synthesis

111-34-2
243 suppliers
$14.00/25mL

7078-90-2 Synthesis

(5-BROMO-2-METHOXY-BENZYL)-DIMETHYL-AMINE

7078-90-2
27 suppliers
inquiry

1-(3-DIMETHYLAMINOMETHYL-4-METHOXY-PHENYL)-ETHANONE

505070-85-9
12 suppliers
inquiry

Yield:505070-85-9 42%

Reaction Conditions:

Stage #1: -butyl vinyl ether;(5-bromo-2-methoxybenzyl)dimethylaminewith palladium diacetate;1,3-bis-(diphenylphosphino)propane;potassium carbonate in N,N-dimethyl-formamide at 80;
Stage #2: with hydrogenchloride in N,N-dimethyl-formamide; for 1 h;

References:

Nielsen, Simon F.;Larsen, Mogens;Boesen, Thomas;Sch?nning, Kristian;Kromann, Hasse [Journal of Medicinal Chemistry,2005,vol. 48,# 7,p. 2667 - 2677]

628-81-9
73 suppliers
$43.75/5G

7078-90-2 Synthesis

7078-90-2
27 suppliers
inquiry

505070-85-9
12 suppliers
inquiry

References

7017-52-9 Synthesis

4-BROMO-2-(CHLOROMETHYL)-1-METHOXYBENZENE

7017-52-9
23 suppliers
inquiry

505070-85-9
12 suppliers
inquiry

References

80866-82-6 Synthesis

80866-82-6
142 suppliers
$18.00/1g

505070-85-9
12 suppliers
inquiry

References

25016-01-7
230 suppliers
$6.00/5g

505070-85-9
12 suppliers
inquiry

References