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ChemicalBook CAS DataBase List 5-Hydroxy-7-Methoxy-2,2-diMethyl-4H-1,3-benzodioxin-4-one

5-Hydroxy-7-Methoxy-2,2-diMethyl-4H-1,3-benzodioxin-4-one synthesis

4synthesis methods
-

Yield:532394-23-3 98%

Reaction Conditions:

with triphenylphosphine;diethylazodicarboxylate in tetrahydrofuran at 0; for 4 h;Mitsunobu reaction;

References:

Chakraborty, Tushar Kanti;Chattopadhyay, Amit Kumar [Journal of Organic Chemistry,2008,vol. 73,# 9,p. 3578 - 3581]