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N,N'-(2-Chloroethylidene)biscarbamic acid diethyl ester synthesis

15synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 87.6 percent / aq. sodium sulfite / 2 h / 15 - 20 °C
2: 90 percent / HCl / diethyl ether / 0.5 h

References:

Bal'on, Ya. G.;Paranyuk, V. E. [Journal of Organic Chemistry USSR (English Translation),1980,vol. 16,p. 1910 - 1914][Zhurnal Organicheskoi Khimii,1980,vol. 16,# 11,p. 2246 - 2251]