ChemicalBook CAS DataBase List Hydrazinecarboxylic acid, 2-(phenylmethyl)-, 1,1-dimethylethyl ester

Hydrazinecarboxylic acid, 2-(phenylmethyl)-, 1,1-dimethylethyl ester synthesis

9synthesis methods

Product Name:Hydrazinecarboxylic acid, 2-(phenylmethyl)-, 1,1-dimethylethyl ester
CAS Number:53370-84-6
Molecular formula:C12H18N2O2
Molecular Weight:222.28

24469-50-9 Synthesis

N'-BENZYLIDENE-HYDRAZINECARBOXYLIC ACID TERT-BUTYL ESTER

24469-50-9
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Hydrazinecarboxylic acid, 2-(phenylmethyl)-, 1,1-dimethylethyl ester

53370-84-6
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Yield:53370-84-6 93%

Reaction Conditions:

Stage #1: N'-(phenylmethylene)hydrazinecarboxylic acid tert-butyl esterwith sodium cyanoborohydride;acetic acid in tetrahydrofuran at 20;
Stage #2: with sodium hydroxide in methanol; for 1 h;Heating;

References:

Weber, Dirk;Berger, Claudia;Eickelmann, Peter;Antel, Jochen;Kessler, Horst [Journal of Medicinal Chemistry,2003,vol. 46,# 10,p. 1918 - 1930]

24469-50-9 Synthesis

24469-50-9
44 suppliers
$33.00/250mg

53370-84-6
15 suppliers
inquiry

References

870-46-2 Synthesis