3-Furancarboxylic acid, 5-(chloromethyl)-2-methyl-, ethyl ester synthesis

4synthesis methods

Product Name:3-Furancarboxylic acid, 5-(chloromethyl)-2-methyl-, ethyl ester
CAS Number:53582-51-7
Molecular formula:C9H11ClO3
Molecular Weight:202.63

3-Furancarboxylicacid, 5-formyl-2-methyl-, ethyl ester

19615-48-6
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3-Furancarboxylic acid, 5-(chloromethyl)-2-methyl-, ethyl ester

53582-51-7
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium tetrahydroborate / 0.5 h
2: N-chloro-succinimide; dimethylsulfide / dichloromethane / 1 h / -20 - 5 °C / Inert atmosphere

References:

Elias-Rodriguez, Pilar;Moreno-Clavijo, Elena;Carmona, Ana T.;Moreno-Vargas, Antonio J.;Robina, Inmaculada [Organic and Biomolecular Chemistry,2014,vol. 12,# 31,p. 5898 - 5904]

3-Furancarboxylic acid, 5-(hydroxymethyl)-2-methyl-, ethyl ester

15341-70-5
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53582-51-7
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References

3-Furancarboxylic acid, 2-methyl-5-[(1S,2R,3R)-1,2,3,4-tetrahydroxybutyl]-, ethyl ester

3351-43-7
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53582-51-7
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References

2-METHYL-3-FURANCARBOXYLIC ACID ETHYL ESTER

28921-35-9
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$45.00/50mg

50-00-0 Synthesis

50-00-0
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$10.00/25g

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References