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ChemicalBook CAS DataBase List 5-BENZYLOXY-1H-INDOLE-2-CARBOXYLIC ACID METHYL ESTER

5-BENZYLOXY-1H-INDOLE-2-CARBOXYLIC ACID METHYL ESTER synthesis

12synthesis methods
Benzenamine, 2-(2,2-dibromoethenyl)-4-(phenylmethoxy)-

863870-46-6
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201230-82-2 Synthesis
carbon monoxide

201230-82-2
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Yield:55581-41-4 72%

Reaction Conditions:

with bis-triphenylphosphine-palladium(II) chloride;N-ethyl-N,N-diisopropylamine;triphenylphosphine in tetrahydrofuran at 110; under 7600.51 Torr; for 20 h;Autoclave;

References:

Vieira, Tiago O.;Meaney, Laura A.;Shi, Yong-Ling;Alper, Howard [Organic Letters,2008,vol. 10,# 21,p. 4899 - 4901] Location in patent:supporting information; experimental part