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Carbamic acid, [1-(2-hydroxyethyl)-4-piperidinyl]-, 1,1-dimethylethyl ester (9CI) synthesis

1synthesis methods
-

Yield:558443-53-1 100%

Reaction Conditions:

with potassium carbonate in acetonitrile; for 5 h;Inert atmosphere;Reflux;

References:

Yang, Katherine S.;Budin, Ghyslain;Reiner, Thomas;Vinegoni, Claudio;Weissleder, Ralph [Angewandte Chemie - International Edition,2012,vol. 51,# 27,p. 6598 - 6603] Location in patent:supporting information; experimental part