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ChemicalBook CAS DataBase List (4S)-4α-[(Z)-2-(3-Furyl)vinyl]-4a,5,6,7,8,8aβ-hexahydro-3,4aα,8,8-tetramethylnaphthalen-1(4H)-one
56324-54-0

(4S)-4α-[(Z)-2-(3-Furyl)vinyl]-4a,5,6,7,8,8aβ-hexahydro-3,4aα,8,8-tetramethylnaphthalen-1(4H)-one synthesis

9synthesis methods
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 90 percent / 2,4,6-collidine / 2 h / 160 °C
2: -78 °C
3: 2,6-lutidine; MsCl / CH2Cl2

References:

Aslaoui, Jamila;Li, Haibing;Morin, Christophe [Tetrahedron Letters,2005,vol. 46,# 10,p. 1713 - 1716]

(4S)-4α-[(Z)-2-(3-Furyl)vinyl]-4a,5,6,7,8,8aβ-hexahydro-3,4aα,8,8-tetramethylnaphthalen-1(4H)-one Related Search: