N'-[5-(4-CHLOROBENZOYL)-1,3-THIAZOL-2-YL]-N,N-DIMETHYLIMINOFORMAMIDE synthesis
1synthesis methods
- Product Name:N'-[5-(4-CHLOROBENZOYL)-1,3-THIAZOL-2-YL]-N,N-DIMETHYLIMINOFORMAMIDE
- CAS Number:569350-52-3
- Molecular formula:C13H12ClN3OS
- Molecular Weight:293.77
Yield:569350-52-3 82%
Reaction Conditions:
Stage #1: 4-chlorobenzoylmethyl bromide;1,3-Bis-[1-dimethylamino-meth-(E)-ylidene]-thiourea in dichloromethane at 20; for 0.25 h;
Stage #2: with triethylamine in dichloromethane; for 20 h;
References:
Landreau, Cyrille;Deniaud, David;Meslin, Jean Claude [Journal of Organic Chemistry,2003,vol. 68,# 12,p. 4912 - 4917]