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1-(benzo[d][1,3]dioxol-5-yl)-N,N-dimethylmethanamine synthesis

14synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 100 percent / H2O / 3 h / 23 °C
2: LiALH4 / diethyl ether / 1.17 h / Heating
3: 65 percent / (aq) NaOH / diethyl ether / 1.83 h / -6 °C

References:

Cushman, Mark;Choong, Tung-Chung;Valko, Joseph T.;Koleck, Mary P. [Journal of Organic Chemistry,1980,vol. 45,# 25,p. 5067 - 5073]